5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole

Base Information

• Chemical Name: 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole
• CAS No.: 1224600-70-7
• Molecular Formula: C₁₉H₂₀Cl₂N₄S
• Molecular Weight: 407.367

Synonyms:5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole

Chemical Property of 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole

Chemical Property:

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Technology Process of 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole

There total 1 articles about 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

2,6-dichlorobenzaldehyde (83-38-5) + 4-amino-3-mercapto-5-[1-(tricyclo[3.3.1.13,7]decane)]-4(H)-1,2,4-triazole (151017-99-1) → 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole (1224600-70-7)

Guidance literature:

In ethanol; for 5h; Reflux;

DOI:10.3390/molecules15042526

Reference yield: 86.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole (1224600-70-7) + 1-(3-Trifluoromethylphenyl)piperazine (15532-75-9) → 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-2-[4-(3-trifluoromethylphenyl)-1-piperazinylmethyl]-1,2,4-triazole-3-thione (1224600-88-7)

Guidance literature:

In ethanol; at 20 ℃; Reflux;

DOI:10.3390/molecules15042526

Reference yield: 85.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-3-mercapto-1,2,4-triazole (1224600-70-7) + 1-(4-Fluorophenyl)piperazine (2252-63-3) → 5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-2-[4-(4-fluorophenyl)-1-piperazinylmethyl]-1,2,4-triazole-3-thione (1224600-87-6)

Guidance literature:

In ethanol; at 20 ℃; Reflux;

DOI:10.3390/molecules15042526

upstream raw materials:

2,6-dichlorobenzaldehyde

4-amino-3-mercapto-5-[1-(tricyclo[3.3.1.1^3,7]decane)]-4(H)-1,2,4-triazole

Downstream raw materials:

5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-2-(4-methyl-1-piperazinylmethyl)-1,2,4-triazole-3-thione

5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-2-(4-ethyl-1-piperazinylmethyl)-1,2,4-triazole-3-thione

5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-2-(4-ethoxycarbonyl-1-piperidylmethyl)-1,2,4-triazole-3-thione

5-(1-adamantyl)-4-(2,6-dichlorobenzylideneamino)-2-(4-ethoxycarbonyl-1-piperazinylmethyl)-1,2,4-triazole-3-thione

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