3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester

Base Information

Chemical Name:3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester
CAS No.:188663-00-5
Molecular Formula:C₁₉H₃₄O₃
Molecular Weight:310.477
Hs Code.:

Synonyms:3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester

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Chemical Property of 3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester

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Technology Process of 3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester

There total 4 articles about 3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 674-82-8,2130-41-8
4-methyleneoxetan-2-one

: 188662-98-8
(1R,2S,5R)-5-Methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexanol

: 188663-00-5
3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester

Guidance literature:: With sodium acetate; In acetonitrile; for 2h; Heating;
DOI:10.1016/S0040-4020(97)00002-1

Reference yield:

: 630-17-1
2,2-dimethylpropyl bromide

: 188663-00-5
3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg, 2.) CuI / 1.) Et₂O, reflux, 1 h, 2.) Et₂O, -20 deg C, 6 h; warm to room temperature, overnight; reflux, 4 h

2: 52 percent / Na / toluene; propan-2-ol / 20 h / Heating

3: 86 percent / NaOAc / acetonitrile / 2 h / Heating

With copper(l) iodide; sodium acetate; sodium; magnesium; In isopropyl alcohol; toluene; acetonitrile;
DOI:10.1016/S0040-4020(97)00002-1

Reference yield:

: 89-82-7,90449-51-7
pulegone

: 188663-00-5
3-Oxo-butyric acid (1R,2S,5R)-5-methyl-2-(1,1,3,3-tetramethyl-butyl)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg, 2.) CuI / 1.) Et₂O, reflux, 1 h, 2.) Et₂O, -20 deg C, 6 h; warm to room temperature, overnight; reflux, 4 h

2: 52 percent / Na / toluene; propan-2-ol / 20 h / Heating

3: 86 percent / NaOAc / acetonitrile / 2 h / Heating

With copper(l) iodide; sodium acetate; sodium; magnesium; In isopropyl alcohol; toluene; acetonitrile;
DOI:10.1016/S0040-4020(97)00002-1