Technology Process of Stibanylidynezirconium
There total 7 articles about Stibanylidynezirconium which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
melt;
mixt. of elements pressed to pellet, arc-melted and annealed in evacuated silica tube for 10 d at 800°C; melted in high-frequency furnace and cooled to room temp. within one min;
- Guidance literature:
-
In
neat (no solvent);
by arc-melting the elements (under Ar) and annealing the product (open Ta crucible, sealed in fused silica jacket under Ar); phases formed are identified by powder X-ray diffraction;
DOI:10.1016/0022-4596(88)90130-2
- Guidance literature:
-
In
neat (no solvent);
antimony is volatized from ZrSb2 at 1000°C under dynamic vac.; the initial products after 1 d are Zr2Sb3 and rhombic ZrSb; after further evapn. (2 d) ZrSb is found in both the cubic FeSi and the rhombic structures; phases formed are identified by powder X-ray diffraction;
DOI:10.1016/0022-4596(88)90130-2
