dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate

Base Information

Chemical Name:dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate
CAS No.:532986-71-3
Molecular Formula:C₃₄H₄₄NO₈P
Molecular Weight:625.699
Hs Code.:

Synonyms:dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate

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Chemical Property of dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate

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Technology Process of dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate

There total 9 articles about dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532986-70-2
dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphite

: 532986-71-3
dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/S0968-0896(02)00381-4

Reference yield:

: 130697-96-0
methyl amino(3-hydroxyphenyl)acetate

: 532986-71-3
dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / NaHCO₃ / tetrahydrofuran / 0.5 h / 0 °C

2: K₂CO₃ / acetone / 8 h / Heating

3: 79 percent / LiBH₄ / tetrahydrofuran / 18 h / 0 - 20 °C

4: H₂ / 10 percent Pd-C / ethanol / 2 h / 20 °C / atmospheric pressure

5: KI; K₂CO₃ / dimethylformamide / 48 h / 20 °C

6: tetrazole / acetonitrile / 3 h / 20 °C

7: m-CPBA / CH₂Cl₂ / 0.5 h / 0 °C

With 1H-tetrazole; lithium borohydride; hydrogen; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0968-0896(02)00381-4

Reference yield:

: 111-64-8
n-octanoic acid chloride

: 532986-71-3
dibenzyl 2-(3-ethoxycarbonylmethyloxyphenyl)-2-(octanoylamino)ethyl phosphate

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / NaHCO₃ / tetrahydrofuran / 0.5 h / 0 °C

2: K₂CO₃ / acetone / 8 h / Heating

3: 79 percent / LiBH₄ / tetrahydrofuran / 18 h / 0 - 20 °C

4: H₂ / 10 percent Pd-C / ethanol / 2 h / 20 °C / atmospheric pressure

5: KI; K₂CO₃ / dimethylformamide / 48 h / 20 °C

6: tetrazole / acetonitrile / 3 h / 20 °C

7: m-CPBA / CH₂Cl₂ / 0.5 h / 0 °C

With 1H-tetrazole; lithium borohydride; hydrogen; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/S0968-0896(02)00381-4