methyl amino(3-hydroxyphenyl)acetate

Base Information

• Chemical Name: methyl amino(3-hydroxyphenyl)acetate
• CAS No.: 130697-96-0
• Molecular Formula: C₉H₁₁NO₃
• Molecular Weight: 181.191
• Mol file: 130697-96-0.mol

Synonyms:methyl amino(3-hydroxyphenyl)acetate

Chemical Property of methyl amino(3-hydroxyphenyl)acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of methyl amino(3-hydroxyphenyl)acetate

There total 5 articles about methyl amino(3-hydroxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

methanol (67-56-1) + D-2-hydroxy-1-<3-(allyloxy)phenyl>ethyl azide (169825-25-6) → 3-hydroxyphenylglycine methyl ester (130697-96-0)

Guidance literature:

With tin(ll) chloride; for 20h; Ambient temperature;

DOI:10.1021/jo961412m

Reference yield:

methanol (67-56-1) + D-α-amino-m-hydroxyphenylacetic acid (31932-87-3) → methyl amino(3-hydroxyphenyl)acetate (130697-96-0)

Guidance literature:

With thionyl chloride; at 80 ℃; for 2h;

Reference yield:

(R)-Azido-(3-benzyloxy-phenyl)-acetic acid methyl ester → 3-hydroxyphenylglycine methyl ester (130697-96-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; Yield given; Ambient temperature;

DOI:10.1021/jo00032a028

upstream raw materials:

methanol

D-α-amino-m-hydroxyphenylacetic acid

D-2-hydroxy-1-<3-(allyloxy)phenyl>ethyl azide

(2R,4R)-3-<2-azido-2-<3-(allyloxy)phenyl>-1-oxoethyl>-4-(phenylmethyl)-2-oxazolidinone

Downstream raw materials:

methyl 2-((tert-butoxycarbonyl)amino)-2-(3-hydroxyphenyl)acetate

2-amino-2-(3-hydroxyphenyl)acetamide

tert-butyl (2-hydroxy-1-(3-hydroxyphenyl)ethyl)carbamate

tert-butyl (1-(3-(benzyloxy)phenyl)-2-hydroxyethyl)carbamate