2-(triphenylsilylmethyl)hexanal

Base Information

Chemical Name:2-(triphenylsilylmethyl)hexanal
CAS No.:126741-81-9
Molecular Formula:C₂₅H₂₈OSi
Molecular Weight:372.582
Hs Code.:

Synonyms:2-(triphenylsilylmethyl)hexanal

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Chemical Property of 2-(triphenylsilylmethyl)hexanal

Chemical Property:

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Technology Process of 2-(triphenylsilylmethyl)hexanal

There total 4 articles about 2-(triphenylsilylmethyl)hexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 201230-82-2
carbon monoxide

: 126741-75-1
(Z)-1-(triphenylsilyl)hex-1-ene

: 2-Triphenylsilanyl-heptanal

: 126741-81-9
2-(triphenylsilylmethyl)hexanal

Guidance literature:: With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen; triphenylphosphine; In benzene; at 65 ℃; for 90h; under 20685.9 Torr; Yield given. Yields of byproduct given;

Reference yield:

: 76-86-8
Triphenylsilyl chloride

: 126741-81-9
2-(triphenylsilylmethyl)hexanal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) butyllithium / 1.) hexane, THF, -78 deg C, 2 h, 2.) hexane, THF, RT, 72 h

2: 74 percent / H₂, quinoline / 10percent Pd/CaCO₃ / toluene / 760 Torr / Ambient temperature

3: H₂, carbonylhydridotris(triphenylphosphine)rhodium(I), triphenylphosphine / benzene / 90 h / 65 °C / 20685.9 Torr

With quinoline; carbonylhydridetris(triphenylphosphine)rhodium(I); n-butyllithium; hydrogen; triphenylphosphine; Lindlar's catalyst; In toluene; benzene;

Reference yield:

: 693-02-7
hex-1-yne

: 126741-81-9
2-(triphenylsilylmethyl)hexanal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) butyllithium / 1.) hexane, THF, -78 deg C, 2 h, 2.) hexane, THF, RT, 72 h

2: 74 percent / H₂, quinoline / 10percent Pd/CaCO₃ / toluene / 760 Torr / Ambient temperature

3: H₂, carbonylhydridotris(triphenylphosphine)rhodium(I), triphenylphosphine / benzene / 90 h / 65 °C / 20685.9 Torr

With quinoline; carbonylhydridetris(triphenylphosphine)rhodium(I); n-butyllithium; hydrogen; triphenylphosphine; Lindlar's catalyst; In toluene; benzene;