Boc-ProψPhe-OH

Base Information

Chemical Name:Boc-ProψPhe-OH
CAS No.:103336-10-3
Molecular Formula:C₁₉H₂₇NO₅
Molecular Weight:349.427
Hs Code.:

Synonyms:Boc-ProψPhe-OH

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Chemical Property of Boc-ProψPhe-OH

Chemical Property:

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Technology Process of Boc-ProψPhe-OH

There total 4 articles about Boc-ProψPhe-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42990-55-6,35016-63-8,42990-49-8,16503-53-0
(S)-(alpha)-bromobenzenepropanoic acid

: 103336-10-3
Boc-ProψPhe-OH

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 1,3-dicyclohexylcarbodiimide (DCC) / 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) CH₂Cl₂, overnight

2: 74 percent / NaH / tetrahydrofuran / 3 h / 0 - 10 °C

3: 6 N aq. HCl / 11 h / 100 °C

4: 50percent aq. NaOH / 2-methyl-propan-2-ol / 2.25 h

With hydrogenchloride; sodium hydroxide; sodium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1021/jo00379a019

Reference yield:

: 106163-50-2
(3S,6S)-2-oxo-3-(phenylmethyl)-1-aza-4-oxabicyclo<4.3.0>nonane

: 103336-10-3
Boc-ProψPhe-OH

Guidance literature:: Multi-step reaction with 2 steps

1: 6 N aq. HCl / 11 h / 100 °C

2: 50percent aq. NaOH / 2-methyl-propan-2-ol / 2.25 h

With hydrogenchloride; sodium hydroxide; In tert-butyl alcohol;
DOI:10.1021/jo00379a019

Reference yield:

: 106163-49-9
N-<2-(R)-bromo-3-phenylpropionyl>-L-proline

: 103336-10-3
Boc-ProψPhe-OH

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NaH / tetrahydrofuran / 3 h / 0 - 10 °C

2: 6 N aq. HCl / 11 h / 100 °C

3: 50percent aq. NaOH / 2-methyl-propan-2-ol / 2.25 h

With hydrogenchloride; sodium hydroxide; sodium hydride; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1021/jo00379a019