(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate

Base Information

Chemical Name:(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate
CAS No.:951744-80-2
Molecular Formula:C₃₅H₃₉NO₉
Molecular Weight:617.696
Hs Code.:

Synonyms:(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate

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Chemical Property of (1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate

Chemical Property:

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Technology Process of (1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate

There total 4 articles about (1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27895-95-0
2-bromo-1,2-bis(4-methoxyphenyl)ethanone

: 951744-79-9
4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylic acid

: 951744-80-2
(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

: 177990-33-9
4-Benzyloxycarbonyl-1-tert-butoxycarbonylpiperidine

: 951744-80-2
(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran / 1 h / -78 °C

1.2: -78 - 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

With potassium hexamethylsilazane; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 120-44-5
1,4-di(4-methoxyphenyl)ethanone

: 951744-80-2
(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 4-benzyloxycarbonyl-1-tert-butoxycarbonyl-4-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

With pyridinium hydrobromide perbromide; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;