[N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium

Base Information

Chemical Name:[N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium
CAS No.:1262405-07-1
Molecular Formula:C₂₂H₄₀HfN₂
Molecular Weight:519.992
Hs Code.:

Synonyms:[N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium

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Chemical Property of [N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium

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Technology Process of [N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium

There total 1 articles about [N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.4%

: 1262405-08-2
[N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]triiodohafnium

: 41251-37-0
methyl-d3-magnesium iodide

: 1262405-07-1
[N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium

Guidance literature:: In tetrahydrofuran; diethyl ether; (N2); std. Schlenk technique; soln. of CD3MgI (3 equiv.) in ether was added to soln. of hf complex in THF; stirred for 2 h; filtered; evapd. (vac.); dissolved in hexane; filtered; decanted; washed(cold hexane); dried (vac.); elem. anal.;
DOI:10.1021/om1008742

Reference yield:

: 1262405-07-1
[N-[1,1-dimethyl-2-(ethylimino-κN)propyl]-2,6-bis(1-methylethyl)benzenaminato-κN]tri(methyl-d3)hafnium

: 1262405-12-8
(N-(1,2-dimethyl-2-(ethylamino-κN)propylidene)-2,6-bis(1-methylethyl)benzenaminato-κN)tri(methyl-d3)hafnium

Guidance literature:: In ⁽²⁾H₈-toluene; (N2); std. Schlenk technique; soln. of Hf complex in toluene-d8 was heated at 80°C for 24 h; NMR monitoring; Kinetics;
DOI:10.1021/om1008742