8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1189528-67-3
• Molecular Formula: C₃₆H₃₀BF₅N₂O₂
• Molecular Weight: 628.449
• Mol file: 1189528-67-3.mol

Synonyms:8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 1 articles about 8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

8-(4-trifluoromethylphenyl)-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1357004-01-3) + 4-methoxy-benzaldehyde (123-11-5) → 8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1189528-67-3)

Guidance literature:

Basic conditions;

DOI:10.1039/b911587k

Reference yield: 64.0%

3-(2-methoxyethoxy)prop-1-yne (31995-08-1) + 8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1189528-67-3) → 8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene (1189528-65-1)

Guidance literature:

3-(2-methoxyethoxy)prop-1-yne; With ethylmagnesium bromide; In tetrahydrofuran; at 60 ℃; for 2h;

8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene; In tetrahydrofuran; at 60 ℃; for 12h;

DOI:10.1039/b911587k

upstream raw materials:

8-(4-trifluoromethylphenyl)-1,3,5,7-tetramethyl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

4-methoxy-benzaldehyde

Downstream raw materials:

8-(4-trifluoromethylphenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene