(3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate

Base Information

Chemical Name:(3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate
CAS No.:1285819-59-1
Molecular Formula:C₂₄H₃₁ClN₂O₇S
Molecular Weight:527.038
Hs Code.:

Synonyms:(3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate

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Chemical Property of (3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate

Chemical Property:

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Technology Process of (3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate

There total 4 articles about (3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285819-58-0
4'-chloro-3,4-di(tert-butoxycarbonylamino)benzhydrol

: 124-63-0
methanesulfonyl chloride

: 1285819-60-4
4-(chloro(4-chlorophenyl)methyl)-1,2-di(tert-butoxycarbonylamino)benzene

: 1285819-59-1
(3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.12.057

Reference yield:

: 1285819-57-9
4'-chloro-3,4-di(tert-butoxycarbonylamino)benzophenone

: 1285819-60-4
4-(chloro(4-chlorophenyl)methyl)-1,2-di(tert-butoxycarbonylamino)benzene

: 1285819-59-1
(3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2010.12.057

Reference yield:

: 31431-17-1
4,4'-dichloro-3-nitrobenzophenone

: 1285819-60-4
4-(chloro(4-chlorophenyl)methyl)-1,2-di(tert-butoxycarbonylamino)benzene

: 1285819-59-1
(3,4-bis(tert-butoxycarbonylamino)phenyl)(4-chlorophenyl)methyl methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / N,N-dimethyl-formamide / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 15 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 24 h / 70 °C / Inert atmosphere

4: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C / Inert atmosphere

5: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; sodium azide; palladium 10% on activated carbon; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2010.12.057