2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

Base Information

Chemical Name:2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine
CAS No.:1374263-53-2
Molecular Formula:C₁₈H₂₂BNO₃
Molecular Weight:311.189
Hs Code.:

Synonyms:2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

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Chemical Property of 2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

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Technology Process of 2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

There total 5 articles about 2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88345-93-1
5-bromo-2-(4-methyloxyphenyl)pyridine

: 73183-34-3
bis(pinacol)diborane

: 1374263-53-2
2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 80 ℃; for 65.5h;

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: 5-chloro-2-(4-methoxyphenyl)pyridine

: 1374263-53-2
2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

Guidance literature:: With potassium acetate; XPhos; In 1,4-dioxane; at 80 ℃; for 24h;
DOI:10.1016/j.bmcl.2011.10.037

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1374263-53-2
2-(4-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 24 h / 80 °C

2: potassium acetate; XPhos / 1,4-dioxane / 24 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; sodium carbonate; XPhos; In 1,4-dioxane; ethanol; water; toluene; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.10.037