5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1^3,6.1^8,15.1^7,20.0^9,14.0^23,28]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene

Base Information

• Chemical Name: 5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1^3,6.1^8,15.1^7,20.0^9,14.0^23,28]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene
• CAS No.: 124639-01-6
• Molecular Formula: C₃₂H₂₀N₁₂
• Molecular Weight: 572.591

Synonyms:5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1^3,6.1^8,15.1^7,20.0^9,14.0^23,28]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene

Chemical Property of 5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1^3,6.1^8,15.1^7,20.0^9,14.0^23,28]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene

Chemical Property:

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Technology Process of 5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1^3,6.1^8,15.1^7,20.0^9,14.0^23,28]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene

There total 1 articles about 5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1^3,6.1^8,15.1^7,20.0^9,14.0^23,28]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-diamino-1-phenyl-1,2,4-triazole (14575-59-8) + phthalonitrile (91-15-6) → 8,17-diphenyl-8,17-dihydrodibenzo-5,7,8,10,15,17,18,20-octa-azaporphyrin (124639-02-7) + 5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.13,6.18,15.17,20.09,14.023,28]dotriaconta-1,3,6(32),7,9,11,13,15,17,20(30),21,23,25,27-tetradecaene (124639-01-6)

Guidance literature:

Title compound not separated from byproducts;

Reference yield: 81.0%

5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.13,6.18,15.17,20.09,14.023,28]dotriaconta-1,3,6(32),7,9,11,13,15,17,20(30),21,23,25,27-tetradecaene (124639-01-6) → 29,31-dichlorotitanium-5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.13,6.18,15.17,20.09,14.023,28]dotriaconta-1,3,6(32),7,9,11,13,15,17,20(30),21,23,25,27-tetradecaene

Guidance literature:

With titanium tetrachloride; In nitrobenzene; for 6h; Heating;

DOI:10.1023/A:1024716810867

Reference yield: 81.0%

5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1(3,6).1(8,15).1(17,20).0(9,14).0(23,28)]dotriaconta-1,3,6(32),7,9,11,13,15,17,20(30),21,23,25,27-tetradecaene (124639-01-6) + titanium tetrachloride (7550-45-0) → 29,31-dichlorotitanium-5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1(3,6).1(8,15).1(17,20).0(9,14).0(23,28)]dotriaconta-1,3,6(32),7,9,11,13,15,17,20(30),21,23,25,27-tetradecaene (624748-01-2)

Guidance literature:

In nitrobenzene; byproducts: HCl; mixt. of C20H10N12(C6H5)2, TiCl4 and nitrobenzene heated under reflux for 6 h; ppt. filtered off, washing with benzene and acetone, suspending in 10% HCl, filtration, washing with distd. water, drying at 110°C, treatment with acetone; elem. anal.;

DOI:10.1023/A:1024716810867

upstream raw materials:

3,5-diamino-1-phenyl-1,2,4-triazole

phthalonitrile

Downstream raw materials:

29,31-dichlorotitanium-5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1(3,6).1(8,15).1(17,20).0(9,14).0(23,28)]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene

29,31-dichlorotin-5,19-diphenyl-2,4,5,7,16,18,19,21,29,30,31,32-dodecaazaheptacyclo[20.6.1.1(3,6).1(8,15).1(17,20).0(9,14).0(23,28)]dotriaconta-1,3,6⁽³²⁾,7,9,11,13,15,17,20⁽³⁰⁾,21,23,25,27-tetradecaene

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