Technology Process of trans-1,2-bis(benzoyloxy)-1,2,3,4-tetrahydrodibenz
acridine
There total 7 articles about trans-1,2-bis(benzoyloxy)-1,2,3,4-tetrahydrodibenzacridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 0.5 g / 0.5 h / 260 - 280 °C
2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C
3: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h
4: 1.) t-BuONa, 2.) DDQ / 1.) t-BuOH, reflux, 15 h, 2.) dioxane, reflux, 15 h
5: 83 mg / I2 / benzene / 12 h / Heating
With
ammonia; iodine; sodium; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium t-butanolate;
palladium on activated charcoal;
In
benzene;
DOI:10.1021/jo00382a017
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C
2: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h
3: 1.) t-BuONa, 2.) DDQ / 1.) t-BuOH, reflux, 15 h, 2.) dioxane, reflux, 15 h
4: 83 mg / I2 / benzene / 12 h / Heating
With
ammonia; iodine; sodium; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium t-butanolate;
palladium on activated charcoal;
In
benzene;
DOI:10.1021/jo00382a017
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 0.5 g / 0.5 h / 260 - 280 °C
2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C
3: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h
4: 1.) t-BuONa, 2.) DDQ / 1.) t-BuOH, reflux, 15 h, 2.) dioxane, reflux, 15 h
5: 83 mg / I2 / benzene / 12 h / Heating
With
ammonia; iodine; sodium; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium t-butanolate;
palladium on activated charcoal;
In
benzene;
DOI:10.1021/jo00382a017
