3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde

Base Information

Chemical Name:3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde
CAS No.:1373395-21-1
Molecular Formula:C₂₄H₂₀N₂O₄
Molecular Weight:400.434
Hs Code.:

Synonyms:3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde

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Chemical Property of 3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde

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Technology Process of 3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde

There total 15 articles about 3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1599470-97-9
C₂₄H₂₂N₂O₃

: 1373395-21-1
3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde

Guidance literature:: With nitric acid; In dichloromethane; for 0.25h; Cooling with ice;
DOI:10.1021/jo402749d

Reference yield: 77.0%

: 1373395-20-0
[3-benzyl-4-(4-methoxyphenyl)-1-methyl-1H-benzimidazole-5,6-diyl]dimethanol-2-one

: 1373395-21-1
3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde

Guidance literature:: With N-(tert-butyl)benzenesulfinimidoyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol300704w

Reference yield:

: 1186662-54-3
3-benzyl-4-(4-methoxyphenyl)-3,7,7a,8-tetrahydro-5H-furo-[3,4-f]benzimidazol-5-one

: 1373395-21-1
3-benzyl-4-(4-methoxyphenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[d]imidazole-5,6-dicarbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: manganese(IV) oxide / dichloromethane / 24 h / 20 °C

2: toluene / 24 h / 120 °C

3: sodium hypochlorite / tetrahydrofuran / 0.5 h / 0 - 20 °C

4: diisobutylaluminium hydride / hexane; dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere

5: N-(tert-butyl)benzenesulfinimidoyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

With manganese(IV) oxide; sodium hypochlorite; N-(tert-butyl)benzenesulfinimidoyl chloride; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ol300704w