(η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

Base Information

Chemical Name:(η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate
CAS No.:882534-12-5
Molecular Formula:C₂₂H₃₆FeP₃Si*F₆P
Molecular Weight:622.346
Hs Code.:

Synonyms:(η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

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Chemical Property of (η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

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Technology Process of (η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

There total 1 articles about (η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 882533-99-5
(η5-trimethylsilylcyclopentadienyl)(1-phenyl-4-vinyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

: 1333-74-0
hydrogen

: 882534-12-5
(η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

Guidance literature:: In diethyl ether; ethanol; soln. of iron compd. in mixture of ethanol and methanol containing Pd/C and H2O hydrogenating at roon temp. under 1 atm. for 10 d; filtration, evapn., recrystn. (ethanol) at 4°C, elem. anal.;
DOI:10.1021/ja0578956

Reference yield:

: 110-53-2
1-Bromopentane

: 882534-12-5
(η5-trimethylsilylcyclopentadienyl)(1-ethyl-4-phenyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

: 882534-22-7
(η5-cyclopentadienyl)(1-phenyl-4-pentyl-7-ethyl-1,4,7-triphosphacyclononane)iron(II) hexafluorophosphate

Guidance literature:: With potassium tert-butoxide; (N2); treatment of iron compd. with potassium tert-butoxide and 1-bromopentane;
DOI:10.1021/ja0578956