nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride

Base Information

Chemical Name:nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride
CAS No.:1316665-06-1
Molecular Formula:C₁₈H₁₇NO₅*ClH
Molecular Weight:363.798
Hs Code.:

Synonyms:nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride

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Chemical Property of nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride

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Technology Process of nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride

There total 2 articles about nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 59-67-6
nicotinic acid

: 691860-37-4
2-methoxy-4-vinylphenyl 2-bromoacetate

: 1316665-06-1
nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride

Guidance literature:: nicotinic acid; 2-methoxy-4-vinylphenyl 2-bromoacetate; With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 25 ℃;

With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 0 - 25 ℃;

Reference yield:

: 97-53-0
4-allylguaiacol

: 1316665-06-1
nicotinic acid 4-allyl-2-methoxy-phenoxycarbonylmethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / dichloromethane / 0 - 25 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 25 °C

2.2: 0 - 25 °C

With potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;