methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

Base Information

Chemical Name:methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate
CAS No.:649725-43-9
Molecular Formula:C₁₉H₂₁Br₂NO₄
Molecular Weight:487.188
Hs Code.:

Synonyms:methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

Chemical Property:

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Technology Process of methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

There total 2 articles about methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 649725-42-8
methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

: 649725-43-9
methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

Guidance literature:: With sodium hydrogensulfite; In ethanol; for 48h; Heating / reflux;

Reference yield:

: 219692-15-6
(3,5-dibromo-4-(5-isopropyl-4-methoxy-phenoxy)-phenyl)-acetic acid methyl ester

: 649725-43-9
methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.1 g / nitric acid / benzene / 1 h / 20 °C

2: 457 mg / sodium hydrosulfite / ethanol / 48 h / Heating

With sodium disulfite; nitric acid; In ethanol; benzene;
DOI:10.1016/j.bmcl.2007.05.049

Reference yield:

: 649725-43-9
methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

: 649725-45-1
methyl[3,5-dibromo-4-(3-fluoro-5-isopropyl-4-methoxyphenoxy)phenyl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitrosonium tetrafluoroborate / CH₂Cl₂ / 1 h / 0 °C

1.2: 205 mg / o-xylene / 1 h / Heating

2.1: 210 mg / aq. LiOH / tetrahydrofuran / 20 °C

With lithium hydroxide; nitrosonium tetrafluoroborate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2007.05.049