methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

Base Information

Chemical Name:methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate
CAS No.:649725-42-8
Molecular Formula:C₁₉H₁₉Br₂NO₆
Molecular Weight:517.171
Hs Code.:

Synonyms:methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

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Chemical Property of methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

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Technology Process of methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

There total 1 articles about methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 219692-15-6
(3,5-dibromo-4-(5-isopropyl-4-methoxy-phenoxy)-phenyl)-acetic acid methyl ester

: 649725-42-8
methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

Guidance literature:: (3,5-dibromo-4-(5-isopropyl-4-methoxy-phenoxy)-phenyl)-acetic acid methyl ester; With nitric acid; In water; benzene; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In water; benzene;

Reference yield: 44.0%

: 649725-42-8
methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

: 649725-43-9
methyl[3,5-dibromo-4-(3-amino-5-isopropyl-4-methoxyphenoxy)phenyl]acetate

Guidance literature:: With sodium hydrogensulfite; In ethanol; for 48h; Heating / reflux;

Reference yield:

: 649725-42-8
methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

: 649725-44-0
methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 457 mg / sodium hydrosulfite / ethanol / 48 h / Heating

2.1: nitrosonium tetrafluoroborate / CH₂Cl₂ / 1 h / 0 °C

2.2: 205 mg / o-xylene / 1 h / Heating

With sodium disulfite; nitrosonium tetrafluoroborate; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2007.05.049