[1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride

Base Information

Chemical Name:[1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride
CAS No.:1189140-48-4
Molecular Formula:C₁₄H₉Cl₂N₃O₂
Molecular Weight:322.15
Hs Code.:

Synonyms:[1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride

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Chemical Property of [1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride

Chemical Property:

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Technology Process of [1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride

There total 3 articles about [1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-37-8
oxalyl dichloride

: 154606-56-1
2-chloro-4-(3,5-dimethyl-1H-pyrazol-1-yl)benzonitrile

: 1189140-48-4
[1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride

Guidance literature:: at 80 ℃; for 3h;

Reference yield:

: 67-51-6
3,5-dimethyl-1H-pyrazole

: 1189140-48-4
[1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 1.5 h / 0 °C

2.1: 3 h / 80 °C

With sodium hydride; In N,N-dimethyl-formamide;

Reference yield:

: 60702-69-4
2-chloro-4-fluorobenzonitrile

: 1189140-48-4
[1-(3-chloro-4-cyanophenyl)-3,5-dimethyl-1H-pyrazol-4-yl](oxo)acetyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 1.5 h / 0 °C

2.1: 3 h / 80 °C

With sodium hydride; In N,N-dimethyl-formamide;