methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

Base Information

Chemical Name:methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate
CAS No.:1427330-87-7
Molecular Formula:C₂₂H₁₇F₄NO₃
Molecular Weight:419.375
Hs Code.:

Synonyms:methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

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Chemical Property of methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

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Technology Process of methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

There total 8 articles about methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 67-56-1
methanol

: 1427330-88-8
ethyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

: 1427330-87-7
methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

Guidance literature:: With potassium carbonate; Reflux;

Reference yield:

: 1214382-15-6
C₁₃H₇ClF₂O

: 1427330-87-7
methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: borane-THF / tetrahydrofuran / 2 h / 0 - 60 °C

3: potassium carbonate / Reflux

With borane-THF; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1427330-97-9
3-amino-2 ,4-difluoro-phenol

: 1427330-87-7
methyl 2-[2,4-difluoro-3-[[2-fluoro-5-(3-fluorophenyl)phenyl]methyl amino]phenoxy]acetate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / N,N-dimethyl-formamide / 0.67 h / 20 °C

2: triethylamine / dichloromethane / 3 h / 20 °C

3: borane-THF / tetrahydrofuran / 2 h / 0 - 60 °C

4: potassium carbonate / Reflux

With borane-THF; sodium carbonate; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;