3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl

Base Information

• Chemical Name: 3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl
• CAS No.: 195737-39-4
• Molecular Formula: C₄₂H₃₈O₆
• Molecular Weight: 638.76

Synonyms:3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl

Chemical Property of 3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl

There total 2 articles about 3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

4,4'-diiodo-3,3'-dimethoxylbiphenyl (92160-61-7) + C14H15BO4 (195737-41-8) → 3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl (195737-39-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate;

DOI:10.1021/ja971513h

Reference yield:

3,3'-dimethoxybiphenyl (6161-50-8) → 3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl (195737-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 4 percent / t-BuLi, I₂ / diethyl ether

2: 77 percent / Pd(PPh₃)4, Na₂CO₃

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; tert.-butyl lithium; sodium carbonate; In diethyl ether;

DOI:10.1021/ja971513h

Reference yield:

3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl (195737-39-4) → [1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol (195737-44-1)

Guidance literature:

With boron tribromide;

DOI:10.1021/ja971513h DOI:10.1039/a708841h

upstream raw materials:

4,4'-diiodo-3,3'-dimethoxylbiphenyl

C₁₄H₁₅BO₄

3,3'-dimethoxybiphenyl

Downstream raw materials:

[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

C₇₂H₈₆O₁₈

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