[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

Base Information

Chemical Name:[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol
CAS No.:195737-44-1
Molecular Formula:C₃₆H₂₆O₆
Molecular Weight:554.599
Hs Code.:

Synonyms:[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

Suppliers and Price of [1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

Chemical Property:

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Technology Process of [1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

There total 3 articles about [1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6161-50-8
3,3'-dimethoxybiphenyl

: 195737-44-1
[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

Guidance literature:: Multi-step reaction with 3 steps

1: 4 percent / t-BuLi, I₂ / diethyl ether

2: 77 percent / Pd(PPh₃)4, Na₂CO₃

3: BBr₃

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; tert.-butyl lithium; boron tribromide; sodium carbonate; In diethyl ether;
DOI:10.1021/ja971513h

Reference yield:

: 195737-39-4
3,2',2'',2''',2'''',3'''''-Hexamethoxy-[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']sexiphenyl

: 195737-44-1
[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

Guidance literature:: With boron tribromide;
DOI:10.1021/ja971513h DOI:10.1039/a708841h

Reference yield:

: 92160-61-7
4,4'-diiodo-3,3'-dimethoxylbiphenyl

: 195737-44-1
[1,4';1',1'';4'',4''';1''',1'''';4'''',1''''']Sexiphenyl-3,2',2'',2''',2'''',3'''''-hexaol

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Pd(PPh₃)4, Na₂CO₃

2: BBr₃

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; sodium carbonate;
DOI:10.1021/ja971513h