methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

Base Information

Chemical Name:methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate
CAS No.:73945-34-3
Molecular Formula:C₂₁H₂₈N₂O₄S
Molecular Weight:404.53
Hs Code.:

Synonyms:methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

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Chemical Property of methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

Chemical Property:

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Technology Process of methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

There total 3 articles about methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 73945-35-4
trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

: 73945-34-3
methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

Guidance literature:: In tetrahydrofuran; at 0 ℃;
DOI:10.1021/ja00529a053

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 73945-34-3
methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: 80 percent / tetrahydrofuran / 0 °C

In tetrahydrofuran;
DOI:10.1021/ja00529a053

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 73945-34-3
methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: 80 percent / tetrahydrofuran / 0 °C

In tetrahydrofuran;
DOI:10.1021/ja00529a053