trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

Base Information

Chemical Name:trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid
CAS No.:73945-35-4
Molecular Formula:C₂₀H₂₆N₂O₄S
Molecular Weight:390.503
Hs Code.:

Synonyms:trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

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Chemical Property of trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

Chemical Property:

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Technology Process of trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

There total 1 articles about trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 73945-35-4
trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

Guidance literature:: DOI:10.1021/ja00529a053

Reference yield: 80.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 73945-35-4
trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

: 73945-34-3
methyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate

Guidance literature:: In tetrahydrofuran; at 0 ℃;
DOI:10.1021/ja00529a053

Reference yield:

: 73945-35-4
trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

: 73945-33-2
p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride, pyridine / Ambient temperature

2: 18 percent / triethylamine / dimethylformamide / 1.) 0 deg C, 1 h, 2.) room temperature, 3 h

With pyridine; thionyl chloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00529a053