(1r,4r)-methyl 4-vinylcyclohexanecarboxylate

Base Information

Chemical Name:(1r,4r)-methyl 4-vinylcyclohexanecarboxylate
CAS No.:196399-22-1
Molecular Formula:C₁₀H₁₆O₂
Molecular Weight:168.236
Hs Code.:

Synonyms:(1r,4r)-methyl 4-vinylcyclohexanecarboxylate

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Chemical Property of (1r,4r)-methyl 4-vinylcyclohexanecarboxylate

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Technology Process of (1r,4r)-methyl 4-vinylcyclohexanecarboxylate

There total 5 articles about (1r,4r)-methyl 4-vinylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 54274-80-5
trans-4-formyl-cyclohexanecarboxylic acid methyl ester

: 196399-22-1
(1r,4r)-methyl 4-vinylcyclohexanecarboxylate

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

trans-4-formyl-cyclohexanecarboxylic acid methyl ester; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 189044-30-2
trans-4-vinylcyclohexane carboxylic acid

: 196399-22-1
(1r,4r)-methyl 4-vinylcyclohexanecarboxylate

Guidance literature:: In methanol; for 6h; Heating / reflux;

Reference yield:

: 110928-44-4
trans-(4-hydroxymethyl)cyclohexane-1-carboxylic acid methyl ester

: 196399-22-1
(1r,4r)-methyl 4-vinylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

2.2: 2 h / 0 - 20 °C

With potassium tert-butylate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;