isopropyl hydroxy(4-methylphenyl)acetate

Base Information

Chemical Name:isopropyl hydroxy(4-methylphenyl)acetate
CAS No.:130159-25-0
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:isopropyl hydroxy(4-methylphenyl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl hydroxy(4-methylphenyl)acetate

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Technology Process of isopropyl hydroxy(4-methylphenyl)acetate

There total 6 articles about isopropyl hydroxy(4-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 16208-14-3
2,2-dihydroxy-1-(p-tolyl)ethanone

: 67-63-0,8013-70-5
isopropyl alcohol

: 130159-25-0
isopropyl hydroxy(4-methylphenyl)acetate

Guidance literature:: With ytterbium(III) triflate; at 80 ℃; for 18h;
DOI:10.1021/ol050125e

Reference yield:

: 5524-56-1
ethyl 2-p-tolyl-2-oxoacetate

: 130159-25-0
isopropyl hydroxy(4-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / Inert atmosphere

2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere

4: sodium tetrahydroborate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c4cc00427b