3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde

Base Information

Chemical Name:3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde
CAS No.:1326714-58-2
Molecular Formula:C₁₁H₁₂BrIOS
Molecular Weight:399.09
Hs Code.:

Synonyms:3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde

Chemical Property:

Boiling Point:381.7±42.0 °C(Predicted)
Density:1.84±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Technology Process of 3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde

There total 4 articles about 3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1326714-57-1
3-bromo-2-fluoro-4-iodobenzaldehyde

: 75-66-1
2-methylpropan-2-thiol

: 1326714-58-2
3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 16h; sealed tube;

Reference yield:

: 851368-08-6
1-bromo-2-fluoro-6-iodobenzene

: 1326714-58-2
3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 1 h

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C / sealed tube

With potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 98968-72-0
tert-butyl 2-fluorophenylcarbamate

: 1326714-58-2
3-bromo-2-tert-butylsulfanyl-4-iodobenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 1 h

2.1: hydrogen bromide / ethanol; water / 1.17 h / 20 - 60 °C

2.2: 0.25 h / 0 - 5 °C

2.3: 1 h / 80 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 1 h

4.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C / sealed tube

With hydrogen bromide; tert.-butyl lithium; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;