8-Phenylmenthyl N-glycinate

Base Information

Chemical Name:8-Phenylmenthyl N-glycinate
CAS No.:172267-28-6
Molecular Formula:C₂₁H₃₁NO₂S₂
Molecular Weight:393.615
Hs Code.:

8-Phenylmenthyl N-<bis(methylthio)methylene>glycinate

Synonyms:8-Phenylmenthyl N-glycinate

Suppliers and Price of 8-Phenylmenthyl N-glycinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Phenylmenthyl N-glycinate

Chemical Property:

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Technology Process of 8-Phenylmenthyl N-glycinate

There total 1 articles about 8-Phenylmenthyl N-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-15-0,12122-00-8
carbon disulfide

: 120130-28-1
(-)-8-phenylmenthan-3-yl glycinate

: 74-88-4
methyl iodide

: 172267-28-6
8-Phenylmenthyl N-glycinate

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In benzene; at 20 ℃; for 0.333333h;
DOI:10.1021/jo00129a038

Reference yield:

: 100-39-0
benzyl bromide

: 172267-28-6
8-Phenylmenthyl N-glycinate

: 8-Phenylmenthyl N--D-phenylalaninate

: 8-Phenylmenthyl N--L-phenylalaninate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min;
DOI:10.1021/jo00129a038

Reference yield:

: 105-36-2
ethyl bromoacetate

: 172267-28-6
8-Phenylmenthyl N-glycinate

: 4-Ethyl 8-phenylmenthyl N--L-aspartate

: 4-Ethyl 8-phenylmenthyl N--D-aspartate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min;
DOI:10.1021/jo00129a038