2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl

Base Information

Chemical Name:2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl
CAS No.:92806-40-1
Molecular Formula:C₂₈H₂₆O₄
Molecular Weight:426.512
Hs Code.:

Synonyms:2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl

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Chemical Property of 2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl

Chemical Property:

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Technology Process of 2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl

There total 3 articles about 2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 15519-73-0
2,2'-Dihydroxy-4,4'-dimethylbiphenyl

: 92806-40-1
2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl

Guidance literature:: With iron(III) chloride; In Trichloroethylene; at 50 ℃; for 3h;
DOI:10.1021/jo00092a036

Reference yield:

: 119-61-9
benzophenone

: 106-44-5
p-cresol

: 546-24-7
Pummerer ketone

: 10568-14-6
4-methyl-2-(4-methylphenoxy)phenol

: 15519-73-0
2,2'-Dihydroxy-4,4'-dimethylbiphenyl

: 464-72-2
tetraphenylethane-1,2-diol

: 71128-89-7
2,2',2''-trihydroxy-5,5',5''-trimethyl-m-terphenyl

: 92806-40-1
2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl

Guidance literature:: In acetone; for 18h; Product distribution; Irradiation;

Reference yield:

: 106-44-5
p-cresol

: 92806-40-1
2,2',2,2'''-Tetrahydroxy-5,5',5,5'''-tetramethyl-1,1':3',1:3,1'''-quaterphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 1) AlCl₃, 2) FeCl₃ / 1) CH₃NO₂, 30 min., 2) CH₃NO₂, 25 deg C, 5 h

2: 37 percent / FeCl₃ / nitromethane / 3 h / Ambient temperature

With aluminium trichloride; iron(III) chloride; In nitromethane;
DOI:10.1016/S0040-4020(01)88316-2