Multi-step reaction with 6 steps
1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 20 °C
1.2: 20 °C
2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 5 - 20 °C / Inert atmosphere
3.1: sodium periodate; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride; water / 1,4-dioxane / 0.42 h / 120 °C / Microwave irradiation
4.1: methanol; sodium tetrahydroborate / 1 h / 20 °C
5.1: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 20 °C
6.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 1 h / 60 °C
6.2: 20 °C
With
methanol; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride; water; chloroformic acid ethyl ester; triethylamine; triphenylphosphine; 1,1'-carbonyldiimidazole; lithium hydroxide; diethylazodicarboxylate;
In
tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;