4-phenylcyclohexanone dimethylacetal

Base Information

• Chemical Name: 4-phenylcyclohexanone dimethylacetal
• CAS No.: 136613-01-9
• Molecular Formula: C₁₄H₂₀O₂
• Molecular Weight: 220.312

Synonyms:4-phenylcyclohexanone dimethylacetal

Chemical Property of 4-phenylcyclohexanone dimethylacetal

Chemical Property:

Purity/Quality:

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Technology Process of 4-phenylcyclohexanone dimethylacetal

There total 4 articles about 4-phenylcyclohexanone dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

methanol (67-56-1) + 1-phenyl-4-cyclohexanone (4894-75-1) → 4-phenylcyclohexanone dimethylacetal (136613-01-9)

Guidance literature:

With titanium tetrachloride; triethylamine; In dichloromethane; at 20 ℃; for 0.75h;

DOI:10.1016/S0040-4020(00)01001-2

Reference yield:

1-phenyl-4-cyclohexanone (4894-75-1) + trimethyl orthoformate (149-73-5) → 4-phenylcyclohexanone dimethylacetal (136613-01-9)

Guidance literature:

With Amberlyst 15; In dichloromethane; at 45 ℃; for 0.5h;

Reference yield:

methanol (67-56-1) + 1-phenyl-4-cyclohexanone (4894-75-1) + trimethyl orthoformate (149-73-5) → 4-phenylcyclohexanone dimethylacetal (136613-01-9)

Guidance literature:

With toluene-4-sulfonic acid; at 20 ℃; for 12h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.202107331

upstream raw materials:

methoxytriphenylmethane

1,1-diethylthio-4-phenylcyclohexane

methanol

1-phenyl-4-cyclohexanone

Downstream raw materials:

1-phenyl-1-cyclohexane

4-phenylcyclohexene

4-phenyl-1-methylenecyclohexane

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