Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-⁽²⁾

Base Information

• Chemical Name: Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-⁽²⁾
• CAS No.: 2559-41-3
• Molecular Formula: C₂₄H₂₀F₃N₂O₃P
• Molecular Weight: 472.403
• Mol file: 2559-41-3.mol

Synonyms:Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-⁽²⁾

Chemical Property of Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-⁽²⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-⁽²⁾

There total 1 articles about Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-⁽²⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2-diazo-3-oxo-4,4,4-trifluorobutyrate (18955-75-4) + triphenylphosphine (603-35-0) → Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-(2) (2559-41-3)

Guidance literature:

In di-isopropyl ether;

Reference yield:

Trifluoracetyl-glyoxylsaeure-aethylester-triphenylphosphazin-(2) (2559-41-3) → ethyl 4,4,4-trifluoroacetoacetate (372-31-6)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O; methanol / Heating

2: quinoline / ethanol

With quinoline; In methanol; ethanol; water;

upstream raw materials:

ethyl 2-diazo-3-oxo-4,4,4-trifluorobutyrate

triphenylphosphine

Downstream raw materials:

ethyl 4,4,4-trifluoroacetoacetate