N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol

Base Information

• Chemical Name: N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol
• CAS No.: 1224946-46-6
• Molecular Formula: C₂₅H₃₂N₂O₁₅
• Molecular Weight: 600.533

Synonyms:N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol

Chemical Property of N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol

There total 1 articles about N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-hydroxyethyl)(methyl)amine (109-83-1) + (2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(2-nitro-4-((((4-nitrophenoxy)carbonyl)oxy)methyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate (1188307-60-9) → N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol (1224946-46-6)

Guidance literature:

With dmap; In dichloromethane; at 0 - 25 ℃; Inert atmosphere;

DOI:10.1039/b925070k

Reference yield: 92.0%

N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol (1224946-46-6) + 4-Nitrophenyl chloroformate (7693-46-1) → C32H35N3O19 (1224946-50-2)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 25 ℃; for 1h; Inert atmosphere;

DOI:10.1039/b925070k

Reference yield: 85.0%

phosgene (75-44-5) + N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol (1224946-46-6) → N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol-carbonyl-chloride (1224946-48-8)

Guidance literature:

With triethylamine; In dichloromethane; toluene; at 0 ℃; Inert atmosphere;

DOI:10.1039/b925070k

upstream raw materials:

(2-hydroxyethyl)(methyl)amine

(2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(2-nitro-4-((((4-nitrophenoxy)carbonyl)oxy)methyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Downstream raw materials:

N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol-carbonyl-chloride

C₃₂H₃₅N₃O₁₉

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1224946-46-6 N-methyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-2-aminoethanol

Send

Send

Metric Ton KG G Pound L ML

Send

Send