isonitroso acetanilide-d₅

Base Information

Chemical Name:isonitroso acetanilide-d₅
CAS No.:67580-78-3
Molecular Formula:C₈H₈N₂O₂
Molecular Weight:169.124
Hs Code.:

Synonyms:isonitroso acetanilide-d₅

Suppliers and Price of isonitroso acetanilide-d₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isonitroso acetanilide-d₅

Chemical Property:

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Technology Process of isonitroso acetanilide-d₅

There total 4 articles about isonitroso acetanilide-d₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 302-17-0
chloral hydrate

: 4165-61-1
aniline-d5

: 67580-78-3
isonitroso acetanilide-d₅

Guidance literature:: With sulfuric acid; hydroxylamine hydrochloride; sodium sulfate; In water;
DOI:10.1002/adsc.201600516

Reference yield:

: 1076-43-3
benzene-d6

: 67580-78-3
isonitroso acetanilide-d₅

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; sulfuric acid / 1 h / 20 - 60 °C

2: hydrogen; palladium on activated charcoal / methanol / 24 h / 20 °C / 2585.81 Torr

3: sulfuric acid; sodium sulfate; hydroxylamine hydrochloride / water / 20 °C

With sulfuric acid; palladium on activated charcoal; hydroxylamine hydrochloride; hydrogen; nitric acid; sodium sulfate; In methanol; water;
DOI:10.1039/c6cc04461a

Reference yield:

: 4165-60-0
nitrobenzene-d5

: 67580-78-3
isonitroso acetanilide-d₅

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium on activated charcoal / methanol / 24 h / 20 °C / 2585.81 Torr

2: sulfuric acid; sodium sulfate; hydroxylamine hydrochloride / water / 20 °C

With sulfuric acid; palladium on activated charcoal; hydroxylamine hydrochloride; hydrogen; sodium sulfate; In methanol; water;
DOI:10.1039/c6cc04461a