trans-2,3-bis(4-chlorophenyl)piperazine

Base Information

Chemical Name:trans-2,3-bis(4-chlorophenyl)piperazine
CAS No.:133603-87-9
Molecular Formula:C₁₆H₁₆Cl₂N₂
Molecular Weight:307.222
Hs Code.:

Synonyms:trans-2,3-bis(4-chlorophenyl)piperazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-2,3-bis(4-chlorophenyl)piperazine

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Technology Process of trans-2,3-bis(4-chlorophenyl)piperazine

There total 2 articles about trans-2,3-bis(4-chlorophenyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 60434-95-9
(1E,1'E)-N,N'-(ethane-1,2-diyl)bis(1-(4-chlorophenyl)methanimine)

: 133603-87-9
trans-2,3-bis(4-chlorophenyl)piperazine

Guidance literature:: With manganese; trifluoroacetic acid; In toluene; acetonitrile; at 20 ℃;
DOI:10.1021/ol034469l

Reference yield: 80.0%

: 60434-95-9
N,N'-bis(4-chlorobenzylidene)ethane-1,2-diamine

: 133603-87-9
trans-2,3-bis(4-chlorophenyl)piperazine

Guidance literature:: With titanium(IV) isopropylate; titanium tetrachloride; zinc; In dichloromethane; at 0 - 25 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jo502688b

Reference yield: 53.0%

: 133603-87-9
trans-2,3-bis(4-chlorophenyl)piperazine

: 106-93-4
ethylene dibromide

: 2,3-bis(4-chlorophenyl)-1,4-diazabicyclo[2.2.2]octane

Guidance literature:: With triethylamine; potassium iodide; In acetonitrile; at 80 ℃; for 14h; Inert atmosphere; Cooling;
DOI:10.1021/jo502688b