4[(CH₃)3NCH₂C₆H₅]⁽¹⁺⁾*[Fe₆S₉(SC(CH₃)3)2]^(4-)*CH₃OH=[(CH₃)3NCH₂C₆H₅]4[Fe₆S₉(SC(CH₃)3)2]*CH₃OH

Base Information

• Chemical Name: 4[(CH₃)3NCH₂C₆H₅]⁽¹⁺⁾*[Fe₆S₉(SC(CH₃)3)2]^(4-)*CH₃OH=[(CH₃)3NCH₂C₆H₅]4[Fe₆S₉(SC(CH₃)3)2]*CH₃OH
• CAS No.: 80976-82-5
• Molecular Formula: CH₄O*C₈H₁₈Fe₆S₁₁*4C₁₀H₁₆N
• Molecular Weight: 1435.06

Synonyms:4[(CH₃)3NCH₂C₆H₅]⁽¹⁺⁾*[Fe₆S₉(SC(CH₃)3)2]^(4-)*CH₃OH=[(CH₃)3NCH₂C₆H₅]4[Fe₆S₉(SC(CH₃)3)2]*CH₃OH

Chemical Property of 4[(CH₃)3NCH₂C₆H₅]⁽¹⁺⁾*[Fe₆S₉(SC(CH₃)3)2]^(4-)*CH₃OH=[(CH₃)3NCH₂C₆H₅]4[Fe₆S₉(SC(CH₃)3)2]*CH₃OH

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Technology Process of 4[(CH₃)3NCH₂C₆H₅]⁽¹⁺⁾*[Fe₆S₉(SC(CH₃)3)2]^(4-)*CH₃OH=[(CH₃)3NCH₂C₆H₅]4[Fe₆S₉(SC(CH₃)3)2]*CH₃OH

There total 2 articles about 4[(CH₃)3NCH₂C₆H₅]⁽¹⁺⁾*[Fe₆S₉(SC(CH₃)3)2]^(4-)*CH₃OH=[(CH₃)3NCH₂C₆H₅]4[Fe₆S₉(SC(CH₃)3)2]*CH₃OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

lithium tert-butylsulfide (16203-42-2) + lithium sulfide + lithium methanolate (865-34-9) + iron(III) chloride (7705-08-0) + trimethylbenzylammonium bromide (5350-41-4) → 4[(CH3)3NCH2C6H5](1+)*[Fe6S9(SC(CH3)3)2](4-)*CH3OH=[(CH3)3NCH2C6H5]4[Fe6S9(SC(CH3)3)2]*CH3OH (80976-82-5)

Guidance literature:

In methanol; mixing of FeCl3, Li2S and LiSt-Bu; in excess of LiOMe, under N2, stirring, 55°, 1-2 h; pptn. with Me3NCH2Ph; recrystn. from DMSO/MeOH;

DOI:10.1021/ja00410a071

Reference yield:

lithium sulfide + lithium methanolate (865-34-9) + iron(III) chloride (7705-08-0) + trimethylbenzylammonium bromide (5350-41-4) + 2-methylpropan-2-thiol (75-66-1) → di-tert-butyl disulfide (110-06-5) + 4[(CH3)3NCH2C6H5](1+)*[Fe6S9(SC(CH3)3)2](4-)*CH3OH=[(CH3)3NCH2C6H5]4[Fe6S9(SC(CH3)3)2]*CH3OH (80976-82-5)

Guidance literature:

In methanol; byproducts: LiCl; under N2, to methanol soln. of LiOMe added (CH3)3CSH and filtered soln.of FeCl3 in CH3OH, anhyd. Li2S added to this mixt., heated at 55°C for 1-2 h, stirred overnight at ambient temp., filtered into methanolsoln. of (Me3NCH2Ph)Br; filtered, recrystd. from Me2SO/MeOH (1:1), elem. anal.;

upstream raw materials:

lithium methanolate

iron(III) chloride

trimethylbenzylammonium bromide

2-methylpropan-2-thiol

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