2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

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Chemical Name:2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on
CAS No.:83498-76-4
Molecular Formula:C₃₆H₃₈N₄O₇
Molecular Weight:638.72
Hs Code.:

Synonyms:2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

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Chemical Property of 2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

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Technology Process of 2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

There total 3 articles about 2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72564-99-9
4-Methoxy-2-methylthio-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-7H-pyrrolo<2,3-d>pyrimidin

: 83498-76-4
2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / 0.5 N HCl, 4,4'-thiobis(2-tert-butyl-5-methylphenol / dioxane / 16 h / Heating

2: 1) 20 percent NaH / 1)1,2-dimethoxy ethan, 10 min at room temp.; 2) 1 h

3: 1) 20 percent NaH in parafine / 1) 110 deg C; 2) 30 min. at 110 deg C

With hydrogenchloride; 2,2'-Dimethyl-5,5'-di-tert-butyl-4,4'-dihydroxy-diphenyl-sulfid, Lanotox; sodium hydride; In 1,4-dioxane;
DOI:10.1002/jlac.198219820906

Reference yield:

: 83498-74-2
3,7-Dihydro-2-methylthio-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

: 83498-76-4
2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 20 percent NaH / 1)1,2-dimethoxy ethan, 10 min at room temp.; 2) 1 h

2: 1) 20 percent NaH in parafine / 1) 110 deg C; 2) 30 min. at 110 deg C

With sodium hydride;
DOI:10.1002/jlac.198219820906

Reference yield:

: 60-35-5
acetamide

: 83498-75-3
3,7-Dihydro-3-methoxymethyl-2-methylthio-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

: 83498-76-4
2-Acetamido-3,7-dihydro-3-methoxymethyl-7-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)-4H-pyrrolo<2,3-d>pyrimidin-4-on

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) 110 deg C; 2) 30 min. at 110 deg C;
DOI:10.1002/jlac.198219820906