Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Base Information

Chemical Name:Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid
CAS No.:136408-90-7
Molecular Formula:C₂₁H₂₉NO₇
Molecular Weight:407.464
Hs Code.:

Synonyms:Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

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Chemical Property of Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

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Technology Process of Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

There total 8 articles about Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 136408-89-4
Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid

: 136408-90-7
Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 110 ℃;

Reference yield:

: 54400-75-8
allyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 136408-90-7
Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 93 percent / pyridine / 12 h

3: 50 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 16 h / 0 °C

4: 65 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

5: 69 percent / LiCl, HMPT / 3 h / Heating

6: 53 percent / Bu₃SnH, AIBN / toluene / 110 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; tri-n-butyl-tin hydride; sodium cyanoborohydride; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 136408-90-7
Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 93 percent / pyridine / 12 h

3: 50 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 16 h / 0 °C

4: 65 percent / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

5: 69 percent / LiCl, HMPT / 3 h / Heating

6: 53 percent / Bu₃SnH, AIBN / toluene / 110 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; camphor-10-sulfonic acid; tri-n-butyl-tin hydride; sodium cyanoborohydride; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;