Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid

Base Information

• Chemical Name: Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid
• CAS No.: 136408-89-4
• Molecular Formula: C₂₁H₂₈ClNO₇
• Molecular Weight: 441.909

Synonyms:Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid

Chemical Property of Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid

Chemical Property:

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Technology Process of Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid

There total 8 articles about Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

Allyl-2-acetamido-3-O-acetyl-2-desoxy-6-O-(4-methoxybenzyl)-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid (136408-88-3) → Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid (136408-89-4)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium chloride; for 3h; Heating;

Reference yield: 66.0%

Allyl-2-acetamido-3-O-acetyl-2-desoxy-6-O-(4-methoxybenzyl)-4-O-(methylsulfonyl)-α-D-glucopyranosid (136408-87-2) → Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid (136408-89-4)

Guidance literature:

With lithium chloride; In N,N-dimethyl-formamide; Heating;

Reference yield: 13.0%

Allyl-2-acetamido-3-O-acetyl-2-desoxy-6-O-(4-methoxybenzyl)-α-D-glucopyranosid (136408-82-7) → Allyl-2-acetamido-3-O-acetyl-4-chlor-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-galactopyranosid (136408-89-4)

Guidance literature:

With pyridine; sulfuryl dichloride; at -10 ℃; for 48h;

upstream raw materials:

Allyl-2-acetamido-3-O-acetyl-2-desoxy-6-O-(4-methoxybenzyl)-α-D-glucopyranosid

Allyl-2-acetamido-3-O-acetyl-2-desoxy-6-O-(4-methoxybenzyl)-4-O-(methylsulfonyl)-α-D-glucopyranosid

Allyl-2-acetamido-3-O-acetyl-2-desoxy-6-O-(4-methoxybenzyl)-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

allyl 2-acetamido-2-deoxy-α-D-glucopyranoside

Downstream raw materials:

Allyl-2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

2-acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-D-xylo-hexoseoxim

2-Acetamido-3-O-acetyl-2,4-didesoxy-6-O-(4-methoxybenzyl)-α-D-xylo-hexopyranosid

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