Technology Process of C30H36N6O3
There total 10 articles about C30H36N6O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
palladium diacetate;
In
1,4-dioxane;
at 80 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: titanium(IV) isopropylate / dichloromethane; diethyl ether / 1 h / -60 - 20 °C
1.2: 2 h / 20 °C
2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 48 h / 60 °C
3.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / 1,4-dioxane / 15 h / 80 °C
With
titanium(IV) isopropylate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; N-ethyl-N,N-diisopropylamine;
palladium diacetate;
In
1,4-dioxane; diethyl ether; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / palladium on activated charcoal / ethanol; tetrahydrofuran / 16 h / 760.05 Torr
2: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / 1,4-dioxane / 15 h / 80 °C
With
hydrogen; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;
palladium on activated charcoal; palladium diacetate;
In
tetrahydrofuran; 1,4-dioxane; ethanol;