2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Base Information

Chemical Name:2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside
CAS No.:89499-95-6
Molecular Formula:C₅₅H₅₉FO₁₂S
Molecular Weight:963.131
Hs Code.:

Synonyms:2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

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Chemical Property of 2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

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Technology Process of 2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

There total 5 articles about 2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 89499-94-5
2,3-di-O-benzyl-4,6-di-O-methanesulphonyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

: 89499-95-6
2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In acetonitrile; for 16h; Heating;
DOI:10.1016/0008-6215(84)85160-5

Reference yield:

: 60825-19-6
4,6-O-isopropylidene sucrose hexabenzoate

: 89499-95-6
2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / NaH / dimethylformamide / Ambient temperature

2: 83 percent / H₂O / acetic acid; acetone / 0.5 h / 85 - 90 °C

3: 95 percent / pyridine

4: 80 percent / tetrabutylammonium fluoride / acetonitrile / 16 h / Heating

With tetrabutyl ammonium fluoride; water; sodium hydride; In pyridine; acetic acid; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/0008-6215(84)85160-5

Reference yield:

: 98-88-4
benzoyl chloride

: 89499-95-6
2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine

2: 93 percent / NaH / dimethylformamide / Ambient temperature

3: 83 percent / H₂O / acetic acid; acetone / 0.5 h / 85 - 90 °C

4: 95 percent / pyridine

5: 80 percent / tetrabutylammonium fluoride / acetonitrile / 16 h / Heating

With pyridine; tetrabutyl ammonium fluoride; water; sodium hydride; In pyridine; acetic acid; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/0008-6215(84)85160-5