4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Base Information

Chemical Name:4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside
CAS No.:89499-98-9
Molecular Formula:C₆₁H₆₁FO₁₁
Molecular Weight:989.147
Hs Code.:

Synonyms:4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

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Chemical Property of 4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

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Technology Process of 4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

There total 6 articles about 4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 532-32-1
sodium benzoate

: 89499-95-6
2,3-di-O-benzyl-6-deoxy-6-fluoro-4-O-mesyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

: 89499-98-9
4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; at 100 ℃; for 72h;
DOI:10.1016/0008-6215(84)85160-5

Reference yield:

: 60825-19-6
4,6-O-isopropylidene sucrose hexabenzoate

: 89499-98-9
4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / NaH / dimethylformamide / Ambient temperature

2: 83 percent / H₂O / acetic acid; acetone / 0.5 h / 85 - 90 °C

3: 95 percent / pyridine

4: 80 percent / tetrabutylammonium fluoride / acetonitrile / 16 h / Heating

5: 81 percent / hexamethylphosphoric triamide / 72 h / 100 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrabutyl ammonium fluoride; water; sodium hydride; In pyridine; acetic acid; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/0008-6215(84)85160-5

Reference yield:

: 98-88-4
benzoyl chloride

: 89499-98-9
4-O-benzoyl-2,3-di-O-benzyl-6-deoxy-6-fluoro-α-D-galactopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine

2: 93 percent / NaH / dimethylformamide / Ambient temperature

3: 83 percent / H₂O / acetic acid; acetone / 0.5 h / 85 - 90 °C

4: 95 percent / pyridine

5: 80 percent / tetrabutylammonium fluoride / acetonitrile / 16 h / Heating

6: 81 percent / hexamethylphosphoric triamide / 72 h / 100 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrabutyl ammonium fluoride; water; sodium hydride; In pyridine; acetic acid; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/0008-6215(84)85160-5