3-IODO-4-METHOXYTOLUENE

Base Information

• Chemical Name: 3-IODO-4-METHOXYTOLUENE
• CAS No.: 50597-88-1
• Molecular Formula: C8H9IO
• Molecular Weight: 248.063
• Hs Code.: 2909309090
• Mol file: 50597-88-1.mol

Synonyms:1-Iodo-2-methoxy-5-methylbenzene;2-Iodo-1-methoxy-4-methylbenzene;2-Iodo-4-methylanisole;3-Iodo-4-methoxytoluene;4-Methyl-2-iodoanisole;

Chemical Property of 3-IODO-4-METHOXYTOLUENE

Chemical Property:

• Vapor Pressure: 0.0232mmHg at 25°C
• Melting Point: 28-30°C
• Refractive Index: 1.582
• Boiling Point: 257.6 °C at 760 mmHg
• Flash Point: 109.6 °C
• PSA: 9.23000
• Density: 1.634 g/cm³
• LogP: 2.60820
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Iodo-4-methoxytoluene 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-IODO-4-METHOXYTOLUENE

There total 10 articles about 3-IODO-4-METHOXYTOLUENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.5%

→ 2-iodo-4-methylanisole (50597-88-1)

Guidance literature:

Reference yield: 99.0%

p-methylanizole (104-93-8) → 2-iodo-4-methylanisole (50597-88-1)

Guidance literature:

With ammonium iodide; oxone; In methanol; at 20 ℃; for 20h;

DOI:10.1016/j.tetlet.2004.09.010

Reference yield: 82.0%

Cresidine (120-71-8) → 2-iodo-4-methylanisole (50597-88-1)

Guidance literature:

With toluene-4-sulfonic acid; sodium iodide; In water; acetonitrile; at 10 - 25 ℃; for 2h;

DOI:10.1039/c7cc06211g

upstream raw materials:

p-methylanizole

Cresidine

1,3-diiodo-2-methoxy-5-methylbenzene

pyridine

Downstream raw materials:

3-iodo-4-methoxybenzoic acid

4-methoxy-3-p-tolyloxy-toluene

N-(2-methoxy-5-methylphenyl)benzenesulfonamide

N-(2-methoxy-5-methylphenyl)-4-methylbenzenesulfonamide