1-Methyl-3-p-tolyltriazene

Base Information

• Chemical Name: 1-Methyl-3-p-tolyltriazene
• CAS No.: 21124-13-0
• Molecular Formula: C₈H₁₁N₃
• Molecular Weight: 149.195
• Hs Code.: 29270000
• European Community (EC) Number: 244-223-3
• NSC Number: 183741,106329
• UNII: D41T26MB6M
• DSSTox Substance ID: DTXSID8066680
• Nikkaji Number: J36.536J
• Wikidata: Q27276069
• ChEMBL ID: CHEMBL3251109
• Mol file: 21124-13-0.mol

Synonyms:3-methyl-1-p-tolyltriazene;methyl-4-tolyltriazene;methyl-p-tolytriazene

Chemical Property of 1-Methyl-3-p-tolyltriazene

Chemical Property:

• Vapor Pressure: 0.147mmHg at 25°C
• Melting Point: 75-80 °C(lit.)
• Refractive Index: 1.4690 (estimate)
• Boiling Point: 215.5°Cat760mmHg
• Flash Point: 84.1°C
• PSA: 36.75000
• Density: 1.02g/cm³
• LogP: 2.60400
• Storage Temp.: Refrigerator
• Solubility.: soluble in Ether
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 149.095297364
• Heavy Atom Count: 11
• Complexity: 125

Purity/Quality:

97% ^*data from raw suppliers

3-Methyl-1-p-tolyltriazene ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 20/21/22-40
• Safety Statements: 26-28-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)NN=NC
• Uses: 3-Methyl-1-(p-tolyl)triazene was used for methylation during simultaneous determination of hippuric and o-, m- and p-methylhippuric acids by gas chromatography.

Technology Process of 1-Methyl-3-p-tolyltriazene

There total 12 articles about 1-Methyl-3-p-tolyltriazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H18N4O5 (1407791-36-9) → L-glutamic acid (56-86-0,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6) + 3-methyl-1-p-tolyltriazene (20667-76-9,20667-77-0,21124-13-0)

Guidance literature:

With Pseudomonas sp. E_.C_. 3.4.17.11 carboxypeptidase G₂; In aq. buffer; at 30 ℃; pH=7.3; Kinetics; Enzymatic reaction;

DOI:10.1016/j.bmcl.2012.09.029

Reference yield:

ethanol (64-17-5) + C9H11N3O → 3-methyl-1-p-tolyltriazene (20667-76-9,20667-77-0,21124-13-0) + formic acid ethyl ester (109-94-4)

Guidance literature:

With piperidine; at 25 ℃; Rate constant; Mechanism;

Reference yield:

C9H13N3O → 3-methyl-1-p-tolyltriazene (20667-76-9,20667-77-0,21124-13-0)

Guidance literature:

C₉H₁₃N₃O; With water;

With methylamine;

DOI:10.1016/j.bmc.2017.04.049

upstream raw materials:

4-methylbenzene diazonium

methylamine

p-methylbenzenediazonium chloride

4-methylbenzenediazonium tetrafluoroborate

Downstream raw materials:

3-methyl-7β-phenylacetamidoceph-3-em-4-carboxylic acid methyl ester

3,3,3-Trifluoro-N-methyl-2-trifluoromethyl-thiopropionimidic acid p-tolyl ester

N-methyl-p-toluidine

(R)-1-(3-benzoyl-2-methylpropionyl)-L-proline methyl ester

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