C₂₈H₂₉N₃O₄S₂

Base Information

Chemical Name:C₂₈H₂₉N₃O₄S₂
CAS No.:1623807-98-6
Molecular Formula:C₂₈H₂₉N₃O₄S₂
Molecular Weight:535.688
Hs Code.:

C<sub>28</sub>H<sub>29</sub>N<sub>3</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₈H₂₉N₃O₄S₂

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Chemical Property of C₂₈H₂₉N₃O₄S₂

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Technology Process of C₂₈H₂₉N₃O₄S₂

There total 11 articles about C₂₈H₂₉N₃O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1623807-82-8
4-methyl-N-((3-tosyl-2,3,4,5-tetrahydro-1H-[1,4]diazepino[1,7-a]indol-1-yl)methyl)benzenesulfonamide

: 1623807-98-6
C₂₈H₂₉N₃O₄S₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 12h; Schlenk technique;
DOI:10.1002/anie.201400881

Reference yield:

: 120-72-9
indole

: 1623807-98-6
C₂₈H₂₉N₃O₄S₂

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hydroxide / dimethyl sulfoxide / 20 °C / Schlenk technique

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 24 h / 0 - 20 °C / Schlenk technique

3: copper(I) thiophene-2-carboxylate / toluene / 20 °C / Schlenk technique

4: C₃₂H₆₄O₈Rh₂ / 1,2-dichloro-ethane / 2 h / 80 °C / Inert atmosphere; Schlenk technique

5: sodium cyanoborohydride / 1,2-dichloro-ethane / 12 h / 20 °C / Inert atmosphere; Schlenk technique

6: trifluoroacetic acid / water; dichloromethane / 12 h / 20 °C / Schlenk technique

With copper(I) thiophene-2-carboxylate; di-isopropyl azodicarboxylate; C₃₂H₆₄O₈Rh₂; sodium cyanoborohydride; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene; 6: |Pictet-Spengler Synthesis;
DOI:10.1002/anie.201400881

Reference yield:

: 1623807-43-1
C₂₀H₁₉⁽²⁾HN₂O₂S

: 1623807-98-6
C₂₈H₂₉N₃O₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(I) thiophene-2-carboxylate / toluene / 20 °C / Schlenk technique

2.1: C₃₂H₆₄O₈Rh₂ / 1,2-dichloro-ethane / 2 h / 80 °C / Inert atmosphere; Schlenk technique

2.2: 12 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: trifluoroacetic acid / water; dichloromethane / 12 h / 20 °C / Schlenk technique

With copper(I) thiophene-2-carboxylate; C₃₂H₆₄O₈Rh₂; trifluoroacetic acid; In dichloromethane; water; 1,2-dichloro-ethane; toluene; 3.1: |Pictet-Spengler Synthesis;
DOI:10.1002/anie.201400881