(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

Base Information

Chemical Name:(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde
CAS No.:1620083-10-4
Molecular Formula:C₄₁H₄₀O₈
Molecular Weight:660.764
Hs Code.:

(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

Synonyms:(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

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Chemical Property of (3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

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Technology Process of (3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

There total 4 articles about (3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1620083-09-1
((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methanol

: 1620083-10-4
(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

Guidance literature:: With N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; potassium hydrogencarbonate; In dichloromethane; water; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.06.029

Reference yield:

: 1620083-08-0
(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

: 1620083-10-4
(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 25 °C / Inert atmosphere

2: tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide; potassium hydrogencarbonate / dichloromethane; water / 1 h / 0 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; potassium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2014.06.029

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1620083-10-4
(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 25 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 25 °C / Inert atmosphere

3: tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide; potassium hydrogencarbonate / dichloromethane; water / 1 h / 0 °C / Inert atmosphere

With pyridine; N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; potassium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2014.06.029