diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate

Base Information

Chemical Name:diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate
CAS No.:1620083-11-5
Molecular Formula:C₄₆H₅₁O₁₀P
Molecular Weight:794.879
Hs Code.:

diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate

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Chemical Property of diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate

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Technology Process of diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate

There total 5 articles about diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1620083-10-4
(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

: 183204-00-4
[(diethyloxyphosphinyl)methylidene]triphenylphosphorane

: 1620083-11-5
diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.06.029

Reference yield:

: 1620083-08-0
(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

: 1620083-11-5
diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 25 °C / Inert atmosphere

2: tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide; potassium hydrogencarbonate / dichloromethane; water / 1 h / 0 °C / Inert atmosphere

3: N,N-dimethyl-formamide / 16 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; potassium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.06.029

Reference yield:

: 1620083-09-1
((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methanol

: 1620083-11-5
diethyl (E)-2-((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-1-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)vinylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide; potassium hydrogencarbonate / dichloromethane; water / 1 h / 0 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 16 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; potassium hydrogencarbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.06.029