(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

Base Information

Chemical Name:(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane
CAS No.:1620083-08-0
Molecular Formula:C₅₇H₆₀O₈Si
Molecular Weight:901.184
Hs Code.:

(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

Synonyms:(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

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Chemical Property of (((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

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Technology Process of (((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

There total 1 articles about (((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 956485-08-8
((3aR,5R,6S,6aR)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanol

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1620083-08-0
(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

Guidance literature:: With pyridine; at 25 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.06.029

Reference yield: 66.0%

: 1620083-08-0
(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

: 1620083-09-1
((3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.06.029

Reference yield:

: 1620083-08-0
(((3aR,5R,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxol-5-yl)methoxy)(tert-butyl)diphenylsilane

: 1620083-10-4
(3aR,5S,6S,6aR)-5-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)-dihydro-5H-furo[3,2-d][1,3]dioxole-5-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 25 °C / Inert atmosphere

2: tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide; potassium hydrogencarbonate / dichloromethane; water / 1 h / 0 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; potassium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetlet.2014.06.029