bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate

Base Information

Chemical Name:bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate
CAS No.:1312438-75-7
Molecular Formula:C₄₂H₅₃O₁₀PSi
Molecular Weight:776.936
Hs Code.:

Synonyms:bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate

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Chemical Property of bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate

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Technology Process of bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate

There total 3 articles about bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 17176-77-1
Dibenzyl phosphite

: 1312438-74-6
bis(4-methoxybenzyl) (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

: 1312438-75-7
bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 90 ℃;

Reference yield:

: 1312438-70-2
dimethyl 2-hydroxy-4-methylenepentanedioate

: 1312438-75-7
bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: 1-methyl-1H-imidazole / dichloromethane / 0 - 20 °C

2: oxo[hexa(trifluoroacetato)]tetrazinc / di-isopropyl ether / 80 °C / Molecular sieve

3: potassium carbonate / N,N-dimethyl-formamide / 20 - 90 °C

With 1-methyl-1H-imidazole; potassium carbonate; oxo[hexa(trifluoroacetato)]tetrazinc; In dichloromethane; di-isopropyl ether; N,N-dimethyl-formamide;

Reference yield:

: 1312438-71-3
dimethyl (RS)-2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylenepentanedioate

: 1312438-75-7
bis(4-methoxybenzyl) rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-{[tert-butyl(dimethyl)silyl]oxy}-4-pentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: oxo[hexa(trifluoroacetato)]tetrazinc / di-isopropyl ether / 80 °C / Molecular sieve

2: potassium carbonate / N,N-dimethyl-formamide / 20 - 90 °C

With potassium carbonate; oxo[hexa(trifluoroacetato)]tetrazinc; In di-isopropyl ether; N,N-dimethyl-formamide;